Vivek V. Buwa |
Ph.D. Student |
Ekta Jain |
Indian Oil Research Scholar Department of Chemical Engineering, Indian Institute of Technology Delhi, Hauzkhas, New Delhi 110 016, India. Tel: +91-11-2659 6252 e-mail: ektajain2908@gmail.com |
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Research Topic: Gas-Liquid Distributors for Trickle Bed Reactors | ||||
Trickle bed reactors (TBRs) are widely used in the oil industry in hydro-treating, hydro-cracking and hydro-desulphurization processes. The development of gas-liquid distributors to achieve uniform liquid- and temperature-distribution, and intense gas-liquid contacting is crucial for efficient operation of TBRs. The present research work focusses on measurements of liquid hold-up distribution generated by different distributors that are relevant for industrial trickle bed reactors, and also for development of experimentally verified computational fluid dynamics (CFD) based models to predict the performance of these distributors. The experimentally verified CFD models will be used to optimize the performance of existing gas-liquid distributors and to evolve new distributor designs. | ||||
Distributor I | Distributor II | Distributor III | Distributor IV | |
Photograph of a typical dual-tip voidage probe | ||||
Optmization of gas-liquid distributor design to achieve more uniform liquid distribution | Every peak in the voltage fluctuation graph shows presence of non-conductive fluid in the medium, as seen in the video (above) | |||
In-house developed voidage probes were used to study the morphology of flow through different gas-liquid distributors (left). Image on right shows a representative voltage signal for two different types of gas-liquid distributors. These signals can help in comparing different types of gas-liquid distributors on the basis of their inherent flow-type. | ||||
CFD predictions of liquid distribution, and velocity magnitudes of liquid and gas for flow through standard chimney (left) and standard bubble cap (right) using Eulerian-Eulerian simulations | ||||
Highly time-resolved and intrusive measurement technique- Voidage probes, were used to identify the flow-regimes inside the TBR. Modified voidage sensors were used to study the effect of different gas and liquid flow rates on the flow-regime and dispersion inside the bed. | ||||
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The effect of liquid-distributor configurations (semi-uniform, local and one-sided) was investigated on the radial liquid distribution at different axial locations of TBR and the corresponding measurements were validated using bottom liquid collection method. Further, the ability of ERT to measure time-resolved local liquid distribution was verified using voidage sensors for artificially created pulsing flow. The ERT measurements were performed to quantify the effects of gas and liquid flow rates, and particle size on the local liquid holdup. (Singh et al., 2019) | ||||
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